Characterization and Wet Chemical Synthesis of Magnesium Tartrate Nano Particles

U.M. Lathiya¹ , M.J. Joshi² , P.M. Vyas³

Section:Research Paper, Product Type: Journal-Paper
Vol.12 , Issue.2 , pp.26-33, Apr-2024

Online published on Apr 30, 2024

Copyright © U.M. Lathiya, M.J. Joshi, P.M. Vyas . This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
 

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Abstract :
Magnesium tartrate is having application in purgative and food supplement formulations. Magnesium tartrate nanoparticles are obtained by employing the wet chemical method. Aqueous solutions of MgCl2, tartaric acid, and sodium metasilicate (SMS) solutions are added together in the presence of Triton X-100 surfactant in the desired manner. The SMS helps in the formation of magnesium tartrate products. The powder XRD analysis indicates the orthorhombic nature of the magnesium tartrate nano-particles with the 40.35 nm average crystallite size from Scherrer`s method and 10.90 nm from the W-H (Williamson-Hall) method. The particle size and the morphology of nano-particles are studied by using TEM. The FTIR spectrum confirms the functional groups, viz., C-H, O-H, and C=O in the sample. TGA indicates the thermal stability up to 213o C and then decomposition occurs via different stages. The dielectric analysis is reported on the pellet form of the sample within the range of frequency from 10 Hz to 10 MHz and temperature from 303K to 363K. The variation in both dielectric constant and dielectric loss along with the frequency of applied field suggests decreasing nature in the values as the frequency increases. However, the reverse trend is displayed for the A.C. conductivity with increasing frequency. Various parameters are evaluated from Jonscher’s power law and the CBH (Correlated Barrier Hopping) model for A.C. conductivity is suggested from the analysis.

Key-Words / Index Term :
Magnesium tartrate nanoparticles, powder XRD, TEM, FTIR, TGA, Dielectric Properties.

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