Characterization of a certain Schiff base Cu(II) Complexes using Spectroscopic techniques

Sudhir Sawasiya¹ , Pramod Kumar Malviya²

Section:Research Paper, Product Type: Journal-Paper
Vol.12 , Issue.6 , pp.29-35, Dec-2024

Online published on Dec 31, 2024

Copyright © Sudhir Sawasiya, Pramod Kumar Malviya . This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
 

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Abstract :
The current work examines the characteristics of the Copper complex, which are significant because of their use in biomedicine. Salicylaldehyde Benzoyl Hydrazine (SBH) (L), Cu(L1)2SO4.5H2O (1), Cu(L2)2SO4.5H2O (2) and Cu(L3)2SO4.5H2O (3) are the ligands and complexes, where L1=5-Nitro SBH, L2=5-Methyl SBH and L3=5-Bromo SBH. The Cu(II) complexes of Schiff base have been examined using powder X-ray diffraction and various spectroscopic instruments, including FTIR, UV-Vis, and SEM. Following the discovery of the sample`s crystalline nature using X-ray diffraction studies, Miller indices, the lattice parameter, and the average crystallite size were computed. The findings verifying Nano powder of copper smaller than 40 nm in size. Based on FT-IR and UV-Visible spectroscopy, salicylaldehyde and benzoyl hydrazine are used in the production of the Cu (II) complex. The metal complexes` morphology is provided via SEM examination.

Key-Words / Index Term :
FT-IR, Particle size, SEM, Salicylaldehyde benzoyl hydrazine, UV-Visible XRD

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